By G Pattenden
This product isn't to be had individually, it's only offered as a part of a collection. There are 750 items within the set and those are all bought as one entity. summary: This product isn't really on hand individually, it's only bought as a part of a suite. There are 750 items within the set and those are all bought as one entity
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Scheme 49) Reagents: i, BuLi; ii, Me,CHCH,CHO; iii, TsOH; iv, NaIO,; v, PhMe, reflux Scheme 49 On lithiation, the a-silyl-ketimine (75) reacts with aldehydes and ketones as a regiospecific ethyl methyl ketone aldol equivalent. g. Scheme 50). 83:17 (75) Reagents: i, LDA; ii, w o ; iii, H30+,silica gel Scheme 50 119 T. Mukaiyama, M. Ohshima, and T. Nakatsuka, Chem. , 1983,1207. Y. Ueno, L. D. S. Yadav, and M. Okawara, Chem. , 1983, 831. 121 J. Durman, J. Elliott, A. B. McElroy, and S. , 1983,24,3927 lzz A.
J. Burton and D. G. Cox, J . Am. Chem. , 1983,105,650. S . Martin, R. -F. , 1983,24, 5615. 83 A. S. Kende and P. Fludzinski, J. Org. , 1983,48, 1384. & T. Ishihara, M. Yamana, and T. , 1983,24, 5657. I11... 0 It CF2ClCPh L FJ+,/op(oR)2 II R=Ph Ph (40) 0 Ph (39)R =Ph ( 4 1 ) R =Et Ph (42) Reagents: i, HP(Q)(QR),, Et,N; ii, Bun,CuLi, TMEDA; iii, CH,=CHCH,Br difluoromethyl ketones (43) can be converted into the corresponding 2,2difluoro-enol silyl ethers (44) by treatment with zinc and trimethylsilyl chloride in acetonitrile at 60°C.
Llu G. A . Flynn, J . Org. , 1983,48, 4125. lo7 J. General and Synthetic Methods 28 OH i L -iii O (62) Reagents: i, Ph,P= CH,; ii, H30+;iii, KOBu' Ley and Simpkins have reported an approach to synthetically important vinyl sulphones using Peterson olefination. ll1 Following lithiation, phenylsulphonyl(trimethylsily1)methane reacts smoothly with aldehydes and ketones at -78°C to afford (E/Z)-isomeric mixtures of vinyl sulphones such as (63) directly. Other functional groups such as esters, acetals, epoxides, and silyl ethers are inert under the reaction conditions.
General and synthetic methods Volume 8 by G Pattenden