General and Synthetic Methods Volume 14 by G. Pattenden PDF

By G. Pattenden

ISBN-10: 0851869548

ISBN-13: 9780851869544

ISBN-10: 1847556264

ISBN-13: 9781847556264

Expert Periodical stories supply systematic and special assessment assurance of growth within the significant components of chemical learn. Written by means of specialists of their expert fields the sequence creates a distinct provider for the lively study chemist, delivering ordinary serious in-depth bills of growth specifically parts of chemistry. For over eighty years the Royal Society of Chemistry and its predecessor, the Chemical Society, were publishing reviews charting advancements in chemistry, which initially took the shape of Annual experiences. although, by means of 1967 the entire spectrum of chemistry may well n learn more... summary: professional Periodical studies offer systematic and special evaluation assurance of growth within the significant components of chemical study. Written through specialists of their expert fields the sequence creates a distinct carrier for the energetic study chemist, providing normal serious in-depth bills of development specifically components of chemistry. For over eighty years the Royal Society of Chemistry and its predecessor, the Chemical Society, were publishing stories charting advancements in chemistry, which initially took the shape of Annual reviews. notwithstanding, through 1967 the entire spectrum of chemistry may perhaps n

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46. 47. 48. 49. 50. 51. 52. 53. 54. 55. 56. J. A. 30, 1967. J. V. , 1989,30, 3345. M. Knight, J. Chem. , Chem. , 1989, 1812. A. B. Brandes, S. D. Clark, J. Org. 54, 5849. E. Denmark, G. E. 30, 2469. I. Luengo and M. Koreeda, J. Org. , 1989,54, 5415. R. Ideses and A. Shani, Tetrahedron, 1989,45, 3523. A. Alexakis and D. 45, 381. K. Saigo, K. Kudo, Y. Hashimoto, N. Kihara and M. Hasegawa, Chem. , 1989, 1203. T. Nomoto and H. Takayama,J. Chem. , Chem. , 1989, 295. Ma, Y Yu and X . Lu. J. Org. 54, 1105.

A wide range of functionality is tolerated, no epimerisationof a-stereogenic centres occurs, and over-reduction to alkenes does not appear to be a problem. 78 The organocopper derivatives are prepared in situ from the corresponding zinc derivatives, as shown in the scheme. The range of functionality tolerated and the mildness of the reaction conditions makes this an attractive approach for the preparation of natural products with functionalisedalkenes and alkynes. 2 equiv) and excess carbon tetrachloride.

Catalytic nickel sulphate in the presence of potassium persulphate as re-oxidantconverts allylic alcohols to a@unsaturated aldehydes and ketones. l3 The active species, presumed to be nickel peroxide, does not oxidise saturated alcohols and is selective for primary allylic alcohols over secondary ones. l4 a-Haloaldehydesand ketones are important for their synthetic utility and biological properties, and two reagents have been reported for the oxidation of a-halocarbinols. 16 Other methods for the oxidation of alcohols to aldehydes or ketones reported this year include the use of dimethyl sulphoxide/oxalyl chloride for the direct oxidation of primary trialkylsilylethers to aldehydes [equation (5)],17 the use of the oxammonium salt (4) in the presence of sodium hypochlorite for the selective oxidation of primary alcohols,l8 and two methods using molecular oxygen.

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General and Synthetic Methods Volume 14 by G. Pattenden


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