By Ursula M. Cowgill (auth.), L. R. Pearson, E. L. Grove (eds.)
This quantity offers a suite of papers given on the sixteenth Mid -America Symposium on Spectroscopy held in Chicago, June 14-17, 1965. The Mid-America Symposium is subsidized every year through the Chicago component to the Society for utilized Spectroscopy in cooperation with the St. Louis, Niagara Frontier, Cleveland, Detroit, lndianapolis, and Milwaukee Sections of the Society and the Chicago gasoline Chromatography dialogue crew. even though we consult with this assembly because the Mid-America Symposium, it keeps to draw attendance, curiosity, and inquiry from many components of the area. periods on lnfrared, Raman, Ultraviolet, obvious, Emis sion, Flame, Atomic Absorption, Nuclear Particle, Gamma Ray, Nuclear Magnetic Resonance, X-Ray Spectroscopy, Spec troscopy, Spectrophosphorimetry, and gasoline Chromatography supplied attention-grabbing papers regarding either utilized and theo retical rules. This quantity maintains a sequence of the complaints initiated in 1961 and consists of a suite of 37 papers provided at this assembly. it's the opinion of the Symposium Committee that even if no longer an entire account of the lawsuits, ebook of this assortment as a reference is warranted. As editors of this quantity, we want to show our gratitude to the authors who gave their effort and time in filing their manuscripts in order that this quantity can be released. The Symposium Committee, L. S. grey, W. Baer, Vivian Biske, W. Los eki , M. S. Wang, F. Leahy, J. L. Ogilvie, B. D.
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P)2 a where Ia is the intensity of element a, C a is the weight percent of element a, (fl/ p). is the mass absorption coefficient for the exciting wavelength, (fl/ P)2 is the mass absorption coefficient for the emitted wavelength, and K is a constant. / P)2 is the mass absorption coefficient for the emitted wavelength. 35 for a LiF analyzing crystal. X-RAY FLUORESCENT DETERMlNATION OF MAJOR CONSTITUENTS 49 90 •• 7. :; 60 '" ~ 50 o ~ 40 ~ WI. "t. CI Fig. 2. Uncorrected CI Ka intensity versus concentration.
Simplification, as each element in a multielement complex matrix can be determined individually there is no need to solve simultaneous equations. 4. Reproducibility; as a ratio of X-ray intensities is used instead of absolute intensity, instrument fluctuations or sample changes are compensated for. The technique involves multiplying the intensity of the characteristic fluorescent X-rays by a ratio of the coherent to incoherent scattering of exciting X-rays from the sample. This empirical correction for enhancement and absorption effects has proved to be applicable to matrix effects in simple and complex matrices, thus increasing both speed and accuracy of X-ray analyses.
I~ Ii 0[· '" :. z oz .. '" ~iS X o. OO Fig. 5. 00% copper. 00 40 A. CARNEVALE AND A. J. LINCOLN I. 1 y. 00 1200 Fig. 6. 00% copper. DISCUSSION Since the X-ray procedure developed was to be used as a medium of silver accountability in addition to an in-line production control technique, the reliability of the production specimen submitted for analysis was of considerable concern. A study of linear homogeneity within a production melt during the final casting operation was made using specimen ingots obtained at the beginning, middle, and end of the pouring cycle of a 10,300 troy oz production melt of sterling silver.
Developments in Applied Spectroscopy by Ursula M. Cowgill (auth.), L. R. Pearson, E. L. Grove (eds.)